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Ono, Ayato; Takayanagi, Tomohiro; Sugita, Moe; Ueno, Tomoaki*; Horino, Koki*; Yamamoto, Kazami; Kinsho, Michikazu
JAEA-Technology 2022-036, 31 Pages, 2023/03
JAEA-Technology-2022-036.pdf:8.77MB
In the Japan Atomic Energy Agency (JAEA), many electrical facilities such as power receiving equipment and power supply units are installed in experimental facilities such as the Nuclear Science Research Institute (NSRI) and the Japan Proton Accelerator Research Complex (J-PARC). However, some facilities have been in operation for more than half a century since they were manufactured, some have already been closed or deactivated, and others are still in operation while replacing parts and taking other aging measures. In these facilities, materials that were used because of their excellent properties at the time of manufacture are now designated as hazardous substances and require special management when disposed of. One of them is polychlorinated biphenyl (PCB). PCB were used in a very wide range of fields because of their stability against heat, high electrical insulation, and chemical resistance. However, it was found that PCB have persistent properties and may cause damage to human health and the living environment, and the government has enacted the "Act on Special Measures for Promotion of Proper Treatment of PCB Wastes (PCB Special Measures Law)" to promote reliable and proper disposal. JAEA has almost completed the excavation survey of high-concentration PCB waste and is in the process of excavating low-concentration PCB waste. However, there are still new relevant items to be discovered. This report summarizes and reports the knowledge necessary for identifying PCB waste and points to be noted when handling capacitors, etc., based on examples of actual disassembly and investigation work conducted on power supply units and other electrical equipment, such as capacitors attached to power supply units, etc.
Jitsukata, Shu*; *; ; ; Kurosawa, A.
JNC TN8410 2001-002, 66 Pages, 2000/12
JNC-TN8410-2001-002.pdf:2.03MB
It was required from IAEA to determine a small amount of plutonium in the high active liquid waste solutions (HALW) in the tokai reprocessing plant. High performance spectrophotometer (HPSP), which could be obtained lower detection limit than conventional spectrophotometer, is studied to be applied to the inspection and verification analysis by the IAEA. [Cold Test] Neodymium, showing an absorption peak near the absorption wavelength of plutonium (VI), was used as an alternative element to plutonium, in order to review the calculation method of the peak intensity. As a result, the three-point correction method was found to be simple and effective. [Hot Test] Plutonium nitrate solution was used the fundamental test of this method. Since the method is known to be influenced by acidity, suspended sludge and coexistent elements in a sample, each dependency was examined. It was found that measurement results varied about 14% at a nitric acid concentration of 2-4 mol/L. Sludge should be removed by filtration before the measurement. The effect of coexisting elements could be eliminated adjusting the optical balance between reference and sample beam intensity. In the case of measuring a low concentration plutonium solution sample, a ratio of the peak intensity to the background intensity (S/B ratio) is relatively small. Therefore a method should be improved the S/B ratio by analyzing the obtained spectra. Accumulated average method, moving average method and Fourier transform method was tested. The results showed that a combination of the accumulated average method and the moving average method was the optimum method for the purpose. Linearity of the calibration curve was found between 0-11 mgPu/L. Synthetic sample solution, which simulated the actual constituents of the HALW with plutonium showed a good linear relation at 0-11 mgPu/L. The detection limit for plutonium concentration was 0.07 mgPu/L. When the synthetic HALW solution containing plutonium was measured, the de
-emitters in solutionUsuda, Shigekazu; Sakurai, Satoshi
Radioisotopes, 44(11), p.776 - 784, 1995/11
no abstracts in English
Sumiya, Shuichi; Hayashi, Naomi; ; Narita, Osamu
PNC TN8430 91-001, 45 Pages, 1990/12
A radioanalytical method for low level samarium-151(Sm-151) and promethium-147(Pm-147) in environmental samples has been studied for the environmental assessment around nuclear facilities. In this study, we use the separation method with high performance liquid chromatography (HPLC) to determine Sm-151 and Pm-147 in environmental samples such as sea sediments and marine organisms. Samarium-151 and Pm-147 in environmental samples are coprecipitated with other lanthanoids after adding neodymium(Nd). These nuclides are purified by anion exchange methods in methanol-mineral acid media. After the purification, Sm-151 and Pm-147 are separated with HPLC in lactic acid-sodium hydroxide media, and determined with liquid scintillation counting, respectively. The Nd is determined by inductively coupled plasma atomic emission spectrometry (ICP-AES) to correct chemical recoveries of these nuclides. The detection limits for Sm-151 and Pm-147 in this method are about 0.01Bq/sample.
LatticesMurakami, Kiyonobu; ;
JAERI-M 83-100, 18 Pages, 1983/07
no abstracts in English
; Wadachi, Yoshiki
Nihon Kagakkai-Shi, 1974(4), p.617 - 621, 1974/04
no abstracts in English
Bunseki Kiki, 6(8), p.519 - 523, 1968/00
no abstracts in English
Terashima, Motoki; Saito, Takumi*; Ishii, Tomoko*; Ito, Miki*; Akagi, Yosuke*; Tachi, Yukio
no journal, ,
no abstracts in English
Kusaka, Shota
no journal, ,
Tokai Reprocessing Plant (TRP) is collecting nuclear materials such as spent fuel sheared powder, plutonium and uranium solutions in the process from 2022 as Flush-out, prior to the shift to decontaminating and dismantling. From 22nd March, 2023 to 29th September, 2023, transfer of the plutonium solution to the high active liquid waste storage tanks and rinsing of the equipment were conducted as collecting of plutonium solution. In this presentation, the results of these work will be reported.
